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3-Bromothiophene CAS NO: 872-31-1

3-Bromothiophene CAS NO: 872-31-1

Name: 3-Bromothiophene
CAS NO: 872-31-1
Purity: 97% min
MF: C4H3BrS
MW:163.036
BP:158.4±13.0 °C at 760 mmHg

Name: 3-Bromothiophene   

CAS NO: 872-31-1

Purity: 97% min

MF: C4H3BrS

MW:163.036

BP:158.4±13.0 °C at 760 mmHg

Density:1.7±0.1 g/cm3

MP: -10?C

EINECS:212-821-3

Appearance: Colorless to yellow liquid

Package: 25g, 100g, 500g, bulk package

Application:Pharmaceutical intermediate

 

 

Other name:

Thiophene,3-bromo;

3-thienylBr;

thien-3-yl bromide;

3-thienyl bromide;

3-Bromothiophene    CAS NO: 872-31-1

Application of 3-Bromothiophene   CAS NO: 872-31-1

 

It’蝉 Sulfanilamide antibacterial anti-inflammatory drugs used in the treatment of animal bacterial dysentery bacterial ulcerative enteritis.

 

Preparation of 3-Bromothiophene   CAS NO: 872-31-1

3-Bromothiophene    CAS NO: 872-31-1

 

2,3, 5-tribromothiophene zinc powder acetic acid water and extraction agent were put into the reducing kettle at one time according to the feeding ratio, and stirring was started.  After stirring about 30min, the temperature was raised to reflux and maintained steady reflux for 6~8h, and then sampling analysis was performed to determine whether the reaction reached the end point.

After the reaction, the distillate was first distilled by steam, then the distillate was added to the extractant for extraction, and the extractant was recovered by distillation.Finally, the fractions of 159~161 are received, and the product 3-Bromothiophene   CAS NO: 872-31-1 is obtained .The yield of about 90% .


3-Bromothiophene    CAS NO: 872-31-1

 


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