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Name: 8-Oxa-3-azabicyclo[3.2.1]octane hydrochloride   

CAS NO: 54745-74-3

Purity: 97% min

MF: C6H12ClNO

MW:149.619

BP:N/A

Density:N/A

MP: 197-199 °C

EINECS:N/A

Appearance: asked

Package: 25g, 100g, 500g, bulk package

Application: 365bet娱乐 intermediate

Other name:

8-Oxa-3-azabicyclo[3.2.1]octane;

8-Oxa-3-azabicyclo octane HCl;

8-Oxa-3-azabicyclo[3.2.1]octane--hydrogen chloride ;

Efficient Synthesis of 8-0xa-3-aza-bicyclo(3.2.1)octane Hydrochloride   CAS NO: 54745-74-3

 Aour-step processo generate 8-oxa-3-aza-bicyclo[3.2.1]octaneydrochloridetarting with 5-hydroxymethyl-2-furfuraIdehyde is described.aney nickel-mediatedeductionf 5-hydroxymethyl-2-furfuraldebydefforded 2,5-bis(hydroxymethyl)tetrahydrofuran with predominantlyisonfiguration.onversionfhe diolo ditosylate,ollowedyyclization withenzylamine generatedhe 8-oxa-3-aza-bicyclo[3.2.1]octaneore.heitleompound was prepared viaydrogenolysisfhe N-benzyl group with Pearl-man'satalystnd isolatedsheydrochloridealtromixturef 2-propanolndeptane.heverall yieldorhe process was 43-64%.n impurity generated duringcalepighlightedhe needortrict in-processpecificationorcetonitrileontent prioro performingheinalydrogenolysis. Ethanolonditioningfll processing equipmenthatadcetonitrileontact priorohe introductionfheubstratetockolution isighlyecommended.

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